HDT and Vicat Testing Instruments

Standard-compliant testing to ISO 75, ISO 306, ASTM D1215 and ASTM D648.

ZwickRoell's HDT/Vicat instruments are designed to enable easy, convenient testing in research and development, goods inwards checks and product monitoring, as well as for education and training purposes. 
HDT/Vicat 装置のISO 75 と ISO 306

Overview of HDT and Vicat Testing Instruments

The instruments are available in various versions, with up to 6 measuring stations according to requirements. A connected PC allows convenient test-sequence parameterization and measured-value display (option).

Information Available for Download

熱たわみ温度HDT / Vicat軟化温度ISO 306、ASTM D1525、ISO 75、ASTM D648

Determining the Heat Deflection Temperature

Many plastics applications are placing increasing demands on heat resistance. An important value with regard to the temperature resistance of plastics is the heat deflection temperature. This can be divided into Vicat softening temperature and HDT (heat deflection temperature). In both methods an oil-bath is heated at a defined rate and the temperature is recorded at a deflection or indentation depth specified by the standard.

  • Vicat softening temperature to ISO 306 and ASTM D1525 (VST: Vicat softening temperature)
  • Vicat softening temperature as per ISO 306 and ASTM D1525 as "dry method"
  • Heat deflection temperature ISO 75 ASTM D648 (HDT: Heat deflection / distortion temperature)

Vicat (VST)

Vicat softening temperature (VST) to ISO 306

Test sequence

The indenter is placed on the plastic specimen and loaded with a defined test weight. The specimen is then heated at a specified rate. The VST is obtained when the needle penetrates to a depth of 1 mm. ISO 306 and ASTM D1525 are identical with regard to the test sequence.

  • ISO 306 distinguishes between 2 procedures and 2 different heating rates, totaling 4 different test methods in all:
  • Method A = 10 N load, heating rate 50 K/h
  • Method A = 10 N load, heating rate 120 K/h
  • Method B = 50 N load, heating rate 50 K/h
  • Method B = 50 N load, heating rate 120 K/h

Vicat Dry

Vicat Dry and 'Dry Method'

  • Determination of Vicat softening temperature (VST)
  • of thermoplastics as per ISO 306

Test sequence

Once the heating block has reached the starting temperature, the specimens are positioned in the measuring stations, the instrument is closed pneumatically and the test weight specified in the standards is automatically applied.

On completion of preheating under the influence of force, the displacement signals are zeroed (program-controlled) and warming of the heating block at the preset rate is started. As soon as the required penetration is attained at all stations, the heating is switched off and the test is ended.

Re-cooling is started automatically; the specimens can afterwards be removed.

HDT

Heat deflection temperature to ISO 75 (HDT)

Heat deflection temperature (HDT) indicates the relative behavior of different types of material under load at elevated temperatures. It is determined for materials such as thermoplastics, hard rubber and duroplastic laminates.

Test sequence

A specimen is placed in a 3-point flexure test kit and loaded with the test weight required to achieve the flexural stress specified in the standard. The temperature is then increased at a uniform heating rate of 120K/h. The temperature at which the specimen reaches the deflection specified in the standard is determined.

Test parameters

Deflection
Deflection is specified by ASTM as an absolute deflection of 0.25 mm; ISO standards define an increase in flexural strain of 0.25%.

Specimen positioning
The standard also specifies how the specimen is to be positioned on the anvil: flatwise or edgewise.

Flexural stress
The standards also specify different flexural stresses:

  • ISO
  • Method HDT A: flexural stress = 1.8 MPa
  • Method HDT B: flexural stress = 0.45 MPa
  • Method HDT C: flexural stress = 8.0 MPa
  • ASTM
  • 1.82 MPa and 0.455 MPa
  • Duropl. laminate: 1/1000 of flexural Young's modulus

Test weight
Accurate measurement of specimens before the test, or the use of precisely identical specimens, is therefore extremely important with this method. Use of the standard HDT weight set is only worthwhile if specimen dimensions are adhered to exactly (±0.05 mm). In all other cases the universal set of weights is used.

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